Innovative in Situ Ball Mill for X ray Diffraction
Nov 13, 2017 The renewed interest of mechanochemistry as an ecofriendly synthetic route has inspired original methodologies to probe reactions, with the aim to rationalize unknown mechanisms. Recently, Friščić et al. (Nat. Chem. 2013, 5, 66−73, DOI: 10.1038/nchem.1505) monitored the progress of milling reactions by synchrotron X-ray powder diffraction (XRPD). For the first time, it was possible to ...